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2197鋁鋰合金形變熱處理中T1相的析出行為

發(fā)布人:上海艾荔艾金屬材料有限公司www.85978597.cn 更新時(shí)間:2015-09-28
對(duì)2197鋁鋰合金進(jìn)行形變熱處理,采用HREM高分辨電鏡觀察合金欠時(shí)效和峰時(shí)效兩個(gè)階段的顯微組織,研究T1相析出長(zhǎng)大行為及其界面特征。
2197鋁鋰合金形變熱處理中T1相的析出行為Precipitation behavior of T1 phase duringthermo-mechanical treatment of 2197 Al-Li alloy
對(duì)2197鋁鋰合金進(jìn)行形變熱處理,采用HREM高分辨電鏡觀察合金欠時(shí)效和峰時(shí)效兩個(gè)階段的顯微組織,研究T1相析出長(zhǎng)大行為及其界面特征。結(jié)果表明:形變熱處理2197合金在欠時(shí)效階段主要存在δ′、θ′和T1相,T1相尺寸約為40 nm;峰時(shí)效階段合金中δ′和θ′數(shù)量減少,主要析出相為T1相,其尺寸為50~150 nm,T1相可通過(guò)δ′相的溶解而長(zhǎng)大。在欠時(shí)效和峰時(shí)效兩階段,T1相末端與基體共格,其他區(qū)域與基體非共格。T1相為六方晶系,與基體存在慣析關(guān)系:(0001)T1//(111)A1、[1010]T1//[110]A1,慣析面為{111}A1。
2197 Al-Li alloy was thermo-mechanically treated, and the precipitation and growth of the T1 phase and the phase interface characteristics were studied. The microstructures of thermo-mechanical treated 2197 Al-Li alloy for under-aged and peak-aged states were observed by high resolution electron microscopy (HREM). The results show that during thermo-mechanical treatment, δ′, θ′ and T1 phases are the main phases of under-aged 2197 alloy, the size of T1 phase is about 40 nm. δ′ and θ′ phases number reduce at peak-aged state, while the main phase of peak-aged 2197 alloy is T1 phase with the size of 50-150 nm. The T1 phase grows up by the dissolving of δ′ phase. The end of T1 phase of peak-aged 2197 alloy is coherent with the matrix while the rest is non-coherent during under-aged and peak-aged states. Habit relationships between T1 phase which is hexagonal crystal system and the matrix is as follow: (0001)T1//(111)A1?and [1010]T1//[110]?A1, and the habit plane is {111}A1.
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